SEMESTER LEARNING PLAN
Document can be downloaded here
Course Title: Chemical Speciation
MK code: AKM21 463
Credit Weight: 2
Group of Courts: Elective
Semester: 6
Prerequisite Course: –
Lecturer:
Dr.Muhammad Cholid Djunaidi, S.Si., M.Si.
Nor Basid Adiwibawa Prasetya, S.Si., M.Sc., Ph.D.
Graduate Learning Outcomes (GLO)
| Attitude | GLO1-(S9) | Demonstrate an attitude of responsibility for work in their field of expertise independently. |
| Knowledge | GLO2-(PP1) | Mastering the theoretical concepts of structure, properties, changes, kinetics, and energetics of molecules and chemical systems, identification, separation, characterization, transformation, synthesis of micromolecular chemicals, and their application. |
| GLO3-(PP3) | Mastering the basic principles of software for analysis, synthesis, and molecular modeling in general or more specific chemical fields. | |
| General Skills | GLO4-(KU1) | Able to apply logical, critical, systematic, and innovative thinking in the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise. |
| Special Skills | GLO5-(KK3) | Able to analyze several alternative solutions in identification, analysis, isolation, transformation, and synthesis of available chemicals and present analysis conclusions for appropriate decision making. |
Course Description
In this course, students learn about: In this course, students are given an understanding of the need for speciation, the method of speciation: separation of metal species both in free and organometallic states. Students were introducing to the tandem method (hyphenated techniques/couple techniques) needed to perform speciation. Students are also required to understand the given speciation journals and explain the speciation phenomenon that occurs.
| Week | Expected ability (Sub-CLO) | Study Materials/ Learning Materials | Learning methods | Student Learning Experience | Time (minutes) | Evaluation | |
| Criteria and Indicators | % | ||||||
| 1 | Able to understand (C2), construct (P4), and discuss (A2) Explain the principles and definitions as well as the benefits and methods used to perform speciation | Chemical speciation based on theory, function and definition | Discovery learning
Cooperative learning |
Search, collect and compile existing information to describe the principles of separation of chemistry, physical chemistry, physics, and examples. Discuss and conclude problems/tasks given by lecturers in groups. | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy explains the different principles of speciation and the methods for performing speciation | 5 |
| 2 | Able to understand (C2), construct (P4), and discuss (A2) Describe the definition of tandem technique, examples, and actualization of student knowledge about methods of separation and identification of metals and organometallic | The concept of metal and non-metal speciation | Discovery learning
Cooperative learning |
Discuss and conclude the problems/tasks given by the lecturer in groups. | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy explains Principles of tandem theory: tandem instrumentation of separation and measurement | 5 |
| 3 | Able to understand (C2), construct (P4), and discuss (A2) Describe the definition of separation and tandem techniques, examples, and actualization of students’ knowledge about methods of separation and identification of metals and organometals | Instrumentation theory concept of separation | Discovery learning
Cooperative learning Problem Based Learning |
Discuss and conclude the problems/tasks given by the lecturer in groups. | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy explains Principles of GC and HPLC chromatography theory: application of GC and HPLC to speciation | 5 |
| 4 | Able to understand (C2), construct (P4), and discuss (A2) Describe the definition of tandem technique, examples, and actualization of student knowledge about methods of separation and identification of metals and organometallic | Applications of gas chromatography (GC) and high performance liquid chromatography (HPLC) in chemical speciation | Discovery learning
Cooperative learning Problem Based Learning |
Discuss and conclude the problems/tasks given by the lecturer in groups. | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy of explaining Principles of membrane theory as well as other separation methods for speciation | 5 |
| 5 | Able to understand (C2), construct (P4), and discuss (A2) Principles of speciation theory (chemistry) of arsenic and chromium, some existing arsenic speciation methods, and examine the speciation phenomenon that occurs | Applications of membranes in chemical speciation | Discovery learning
Cooperative learning Problem Based Learning |
Discuss and conclude the problems/tasks given by the lecturer in groups. | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy explains Principle theory – Chemistry of Arsenic and chromium
– Arsenic and chromium speciation method – Examine the phenomenon of speciation |
5 |
| 6 | Able to understand (C2), construct (P4), and discuss (A2) the theory of speciation (chemistry) of selenium, several methods of speciation of selenium and mercury are available and examine the phenomenon of speciation that occurs | Arsenic and chrome speciation | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy explains Principle theory – Selenium and mercury chemistry
– Selenium and mercury speciation method – Examine the phenomenon of selenium speciation |
5 |
| 7 | Able to understand (C2), construct (P4), and discuss speciation applications | Selenium and mercury speciation | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy of explaining the Principle of speciation theory with instrumentation | 10 |
|
8
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|
Midterm exam | Written exam | 90 | The truth and completeness of the answer to the question | ||
| 9 | Able to understand (C2), construct (P4), and discuss (A2) speciation theory (chemistry) based on the pourbaix diagram | Speciation of iron and copper according to the Pourbaix diagram | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
the accuracy of explaining the principle of speciation theory based on the Pourbaix Diagram | 5 |
| 10 | Able to understand (C2), construct (P4), and discuss (A2) separation and speciation using electrophoresis | Study of speciation using electrophoresis: the case of arsenic and selenium | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy of explaining Principles of speciation theory of arsenic and selenium using electrophoresis method | 5 |
| 11 | Able to understand (C2), construct (P4), and discuss (A2) separation and speciation using polarographic techniques | Study of speciation using polarography: the case of tin | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
the accuracy of explaining the principle of tin speciation theory using the polarographic method | 5 |
| 12 | Able to understand (C2), construct (P4), and discuss (A2) The principles of speciation theory (chemical) of cadmium and copper examine the phenomenon of speciation that occurs | Cadmium and copper speciation | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accurately explain the speciation theory of cadmium and copper | 10 |
| 13 | Able to understand (C2), construct (P4), and discuss (A2) separation and speciation using the ion-selective electrode technique | Specific studies using ion-selective electrodes: the case of cadmium and copper | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accurately explain the theoretical principles of cadmium and copper speciation using the ion-selective electrode method | 10 |
| 14 | Able to understand (C2), construct (P4), and discuss (A2) separation and speciation using X-ray spectroscopy techniques | Speciation studies using X-ray spectroscopy | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
the accuracy of explaining the principle of the speciation theory of compounds in solid samples directly using X-ray spectroscopy methods | 10 |
| 15 | Able to understand (C2), construct (P4), and discuss (A2) calibration method in compound speciation method | Internal and external calibration techniques in speciation | Discovery learning
Cooperative learning Problem Based Learning |
Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
accuracy explains the principle of calibration of compound speciation methods using external and internal calibration methods | 5 |
| 16 | Final exams | Written exam | 90 | The truth and completeness of the answer to the question | |||
Reference:
- Kriz, PL,. Introduction to Organic Laboratory Technique
- Sudjadi, 1990, Metode Pemisahan
- Khopkar, 1990, Kimia Analitik Dasar
- Mulder, M, 1996, Basic Principle of Membrane Technology, Kluwer Academic Publisher
- Skoog, 1997, Principle of Instrumental Analytical
- Bartsch, Way, 1996, Chemical Separations with Liquid Membranes, C.S. Symposium Series
- Kot, A., Namiesnik, J. 2000, The role of speciation in analytical chemistry, Trends in Analytical Chemistry, 19, 69-79
- Cornelis, R, 2003, Handbook of elemental speciation: techniques and methodology, John Willey & Sons Ltd, England
Glossary
GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study
