Inorganic Synthesis (SAno)

SEMESTER LEARNING PLAN

Document can be downloaded here

 

Course Title: Inorganic Synthesis (SAno)

MK code: AKM21 458

Credit Weight: 2

Group of Courts: elective

Semester: 5

Prerequisite Course: KAno3

 

Lecturer:

Drs. Suhartana, Msi

Dra. Sriyanti, MS

Pardoyo, SSi. Msi

 

Graduate Learning Outcomes (GLO)

Attitude	GLO1-(S9)	Demonstrate an attitude of responsibility for work in their field of expertise independently.
Knowledge	GLO2-(PP1)	Mastering theoretical concepts about the properties of a compound based on its structure and constituent elements
	GLO2-(PP2)	Mastering complete operational knowledge about functions, how to operate general chemical instruments, and analysis of data and information from these instruments
General Skills	GLO3-(KU1)	Able to apply logical, critical, systematic, and innovative thinking in the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise
Special Skills	GLO4-(KK1)	Able to produce appropriate conclusions based on the identification, analysis, isolation, transformation, and synthesis of chemicals that have been carried out
	GLO5-(KK3)	Able to analyze several alternative solutions in identification, analysis, isolation, transformation, and synthesis of available chemicals and present analysis conclusions for appropriate decision making

 

 

Course Description

This course underlies the courses in inorganic which generally discuss: A brief overview of the Principles of Material Synthesis. The factors that influence it. Application of thermodynamic data for prediction of material synthesis, both spontaneous and kinetic. Synthesis Basic Techniques,The Impact of Solvents on Synthesis. Attempts to increase reaction yield. Inert state manipulation technique in atmospheric conditions. As well as synthesis techniques in a vacuum state. Effect of temperature and catalyst on reaction rate. Temperature measurement settings and techniques at low temperatures. Inert state manipulation technique in atmospheric conditions. As well as synthesis techniques in a vacuum state. Materials synthesis technique using electricity. Examples of synthesis / treatment in several Indonesian factories. Purification of CuSO₄ and NaCl salts, Synthesis of MgSO₄ salts. MgCl₂ salt synthesis, Na₃PO₄ salt synthesis, Na₂SO₄, Na₂CO₃ and NaHPO₄. High Pressure Apparatus, Photochemical Synthesis. Liquid-liquid Extraction. Compound Characterization, Chemical analysis and Elementary Physical Methods. Group discussion, discussing several Material Syntheses in groups, starting with a thermodynamic approach, optimizing results,and analysis of synthesis results (both qualitative and quantitative).

Week	Expected ability (Sub-CLO)	Study Materials/ Learning Materials	Learning methods	Student Learning Experience	Time (minutes)	Evaluation
						Criteria and Indicators	%
1	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about: A brief overview of the Principles of Material Synthesis. Factors that influence it.	Explanation of syllabus and lecture contracts. Introduction: A brief overview of the Principles of Material Synthesis, Factors that affect/accelerate the rate of Material Synthesis.	Discovery learning Cooperative learning	Discussion, describing: Explaining (C2) about a brief overview of the Principles of Material Synthesis. The factors that influence it.	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Brief overview of the Principles of Material Synthesis, Factors that affect it, with an accuracy of at least 80%.	5
2	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about: Application of thermodynamic data for prediction of the synthesis of a material.	Application of thermodynamic data for prediction of the synthesis of a material	Discovery learning Cooperative learning	Discussion, describing: Explaining (C2) Application of thermodynamic data for prediction of the synthesis of a material	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) Application of thermodynamic data for prediction of the synthesis of a material, with a minimum accuracy of 80%,	10
3	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about: Application of Thermodynamic Data for Prediction of kinetic aspects for Material Synthesis	Application of Thermodynamic Data for Prediction of kinetic aspects for Material Synthesis	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Application of thermodynamic data for prediction of the synthesis of a material	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) Application of thermodynamic data for prediction of the synthesis of a material, with a minimum accuracy of 80%,	5
4	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about: Basic Techniques of Synthesis, Impact of Solvents on Synthesis. Attempts to increase reaction yield	Basic Synthetic Techniques	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Basic Techniques of Synthesis, Impact of Solvents on Synthesis. Attempts to increase reaction yield	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2), Basic Synthesis Techniques, Impact of Solvents on Synthesis. Attempts to increase the reaction yield, with an accuracy of at least 80%.	5
5	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about: the effect of temperature on the rate of reaction. Temperature measurement settings and techniques at low temperatures.	Effect of temperature on reaction rate	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) about the effect of temperature on the rate of reaction. Temperature measurement settings and techniques at low temperatures.	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2), about the effect of temperature on the rate of reaction. Temperature measurement settings and techniques at low temperatures. , with an accuracy of at least 80%.	5
6	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about: Inert state manipulation techniques in atmospheric conditions. As well as synthesis techniques in a vacuum state	Manipulation technique of the inactive state in atmospheric conditions. As well as synthesis techniques in a vacuum state	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Inert state manipulation technique in atmospheric conditions. As well as synthesis techniques in a vacuum state.	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Inert state manipulation technique in atmospheric conditions. As well as synthesis techniques in a vacuum state. , with an accuracy of at least 80%.	5
7	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about:Materials Synthesis Techniques using Electricity.	Material Synthesis Techniques using Electricity	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Discussion, describing: Explaining (C2) Material Synthesis Techniques using electricity	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2), Material Synthesis Techniques using electricity, with a minimum accuracy of 80%	5
8		Midterm exam	Written exam		90	The truth and completeness of the answer to the question
9	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1)	Synthesis/treatment at several Indonesian factories. Phosphoric acid manufacture. Manufacture of nitric acid, Manufacture of vinegar, Manufacture of sulfuric acid, and Manufacture of oxalic acid	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2)	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2), with an accuracy of at least 80%	10
10	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about Purification of CuSO4 and NaCl salts, Synthesis of MgSO4 salts. MgCl2 salt synthesis, Na3PO4 salt synthesis, Na2SO4, Na2CO3, and NaHPO4	Purification of CuSO4 and NaCl salts, Synthesis of MgSO4 salts. MgCl2 salt synthesis, Na3PO4 salt synthesis, Na2SO4, Na2CO3, and NaHPO4	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Purification of CuSO4 and NaCl salts, Synthesis of MgSO4 salts. MgCl2 salt synthesis, Na3PO4 salt synthesis, Na2SO4, Na2CO3, and NaHPO4	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Purification of CuSO4 and NaCl salts, Synthesis of MgSO4 salts. MgCl2 salt synthesis, Na3PO4 salt synthesis, Na2SO4, Na2CO3, and NaHPO4  with an accuracy of at least 80%	10
11	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about High-pressure Apparatus, Photochemical Synthesis. Liquid-liquid Extraction	High-pressure Apparatus, Photochemical Synthesis. Liquid-liquid Extraction	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) High-pressure Apparatus, Photochemical Synthesis. Liquid-liquid Extraction	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , High-pressure Apparatus, Photochemical Synthesis. Liquid-liquid Extraction with an accuracy of at least 80%	10
12	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about Compound Characterization, Chemical analysis, and Elementary Physical Methods	Compound Characterization, Chemical analysis, and Elementary Physical Methods	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Compound Characterization, Chemical analysis, and Elementary Physical Methods	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Compound Characterization, Chemical analysis, and Elementary Physical Methods with an accuracy of at least 80%	10
13	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about Compound Characterization, AAS, IR and UV Spectroscopy, XRD and SEM	Compound Characterization, AAS, IR and UV Spectroscopy, XRD and SEM	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Compound Characterization, AAS, IR and UV Spectroscopy, XRD and SEM	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Compound Characterization, AAS, IR and UV Spectroscopy, XRD and SEM with an accuracy of at least 80%	10
14	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis (part I)	Group discussion, discussing several Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis (part I)	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis with an accuracy of at least 80%	5
15	Mastering the theoretical concepts of Natural Science (K1), Able to describe (C1) about Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis (part II)	Group discussion, discussing several Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis (part II)	Discovery learning Cooperative learning Problem Based Learning	Discussion, describing: Explaining (C2) Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis	FF: 1 x (2 x 50”) ST + SS: 1 x [(2 x 50”) + (2 x 60”)]	Accuracy in explaining (C2) , Material Syntheses in groups, starting with a thermodynamic approach, optimizing the results, and analyzing the results of the synthesis with an accuracy of at least 80%	5
16	Final exams			Written exam	90	The truth and completeness of the answer to the question

 

Reference:

1. Jolly WL., The Synthesis and Characterization of Inorganic Compounds, Prentice hall Inc, 1978, New york.
2. Wilberg, KB., 1967, Laboratory technique in Organic Chemistry, Mc Grawhill Book Company, New York.
3. Calvert,JG., and Pitts, JN., 1967. Photochemistry, John Wiley & Sons Inc, New York.

Glossary

GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study