SEMESTER LEARNING PLAN
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Course Title: Organic Analysis (AO)
MK code: AKM21 354
Credit Weight: 2
Group of Courts: Compulsory
Semester: 5
Prerequisite Course: KO3, KOF
Lecturer:
Dr. Khairul Anam. M.Si
Dra. Dewi Kusrini. M.,Si
Ismiyarto, S.Si., M.Si., Ph.D
Graduate Learning Outcomes (GLO)
| Attitude | GLO1-(S9) | Demonstrate an attitude of responsibility for work in their field of expertise independently. |
| Knowledge | GLO2-(PP1) | Mastering the theoretical concepts of structure, properties, changes, kinetics, and energetics of molecules and chemical systems, identification, separation, characterization, transformation, synthesis of micromolecular chemicals and their application |
| GLO3-(PP2) | Mastering complete operational knowledge of functions, how to operate standard chemical instruments, as well as data and information analysis of the instrument | |
| General Skills | GLO4 -(KU1) | Able to apply logical, critical, systematic, and innovative thinking in the context of the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise |
| GLO5 -(KU2) | Able to demonstrate independent, quality, and measurable performance | |
| GLO6 -(KU5) | Able to make decisions regularly in the context of solving problems in their area of expertise, based on the results of information and data analysis | |
| Special skill | GLO7 -(KK1) | Able to produce appropriate conclusions based on the results of identification, analysis, isolation, transformation, and synthesis of chemicals that have been carried out. |
| GLO8 -(KK3) | Able to analyze several alternative solutions in identification, analysis, isolation, transformation, and synthesis of chemicals available and present analysis conclusions for appropriate decision-making. |
Course Description
In this course, students learn about Industrial chemical processes, process engineering, and how to design processes based on the principles they have learned. In the discussion and presentation of assignments using discovery learning, cooperative learning, collaborative learning, and problem-based learning/case studies. The hope in the discussion is that there will be cooperative and collaborative communication between students/groups.
| Week | Expected ability (Sub-CLO) | Study Materials/ Learning Materials | Learning methods | Student Learning Experience | Time (minutes) | Evaluation | |
| Criteria and Indicators | % | ||||||
| 1 | Able to develop a strategy flow for identifying unknown compounds | Systematics of Identification of Organic Compounds | Discovery learning
Cooperative learning |
Students discuss | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
The accuracy of compiling the flow of identification of unknown compounds | 5 |
| 2 | able to understand the emergence of typical physical properties for each organic compound | Identification of Unknown Compounds: a. preliminary test b. physical properties c. solubility test | Discovery learning
Cooperative learning |
Students discuss, presented Task 1 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
Accuracy of describing and predicting physical properties and solubility | 10 |
| 3 | Able to determine the types and quantities of elements that make up organic compounds using simple methods | Elementary analysis of organic compounds qualitatively and quantitatively | Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task2 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
The accuracy of determining the type and amount of the elements that make up the compound is unknown | 10 |
| 4 | Able to determine the weight and molecular formula of organic compounds conventionally | Identification of Unknown Compounds
: d. determination of molecular weight, e. determination of the molecular formula |
Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task3 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
Accuracy determines the molecular formula | 5 |
| 5 | Able to analyze the correlation of physical properties with a molecular structure | Correlation of structure and physical properties:
a. melting point and freezing point b. boiling point |
Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task4 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)]
|
The accuracy of comparing the value of physical properties between organic molecules | 10 |
| 6 | Able to analyze the correlation of physical properties with a molecular structure | Correlation of structure and physical properties:
c. refractive index d. specific gravity e. optical loop |
Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task5 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)]
|
The accuracy of comparing the value of physical properties between organic molecules | 5 |
| 7 | Able to choose purification methods according to the physical properties of unknown compounds | Determination of purity:
a.chromatography b.melting point c.distillate |
Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task6 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)]
|
The accuracy of choosing the purity method | 5 |
|
8
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|
Midterm exam | Written exam | 90 | The truth and completeness of the answer to the question | 50 | |
| 9 | Able to choose separation method according to an unknown physicochemical compound | Organic Compound Separation Methods:
a. extraction b. distillation & sublimation |
Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task7 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
The accuracy of applying the separation method | 5 |
| 10 | Able to choose separation method according to an unknown physicochemical compound | Organic Compound Separation Methods:
c. thin layer chromatography d. HPLC e. GC f. Chromatographic Column |
Discovery learning
Cooperative learning Problem Based Learning |
Students discuss, presenting task 8 | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
The accuracy of applying the separation method | 5 |
| 11 | Able to determine the solubility properties of unknown compounds and be able to predict the type and size of the molecule | Classification of Organic compounds based on solubility:
a. determination of solubility b. solubility theory c. Molecular structure & solubility |
Discovery learning
Cooperative learning Problem Based Learning |
Group discussion describes the solubility properties of unknown compounds and predicts the type of functional group and its molecular size | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
The accuracy of proposing types of chemical structures based on their solubility | 10 |
| 12 | Able to select and determine the type of functional group test according to the physicochemical properties of unknown compounds | Chemical determination of functional groups:
a. acid anhydride b. acyl halide c. alcohol d. aldehyde e. amine |
Discovery learning
Cooperative learning Problem Based Learning |
Discussion of the principle of functional group analysis method | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)] |
The accuracy of applying the test method | 10 |
| 13 | Able to select and determine the type of functional group test according to the physicochemical properties of unknown compounds | Chemical determination of functional groups:
f. carbohydrate g. carboxylic acid h. ester i. ether j. halide k. hydrocarbons |
Discovery learning
Cooperative learning Problem Based Learning |
Discussion of the principle of functional group analysis method | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)]
|
The accuracy of applying the test method | 10 |
| 14 | Able to formulate the right and appropriate strategy flow for the identification of new compounds | Determination of the chemical structure of the new compound | Discovery learning
Cooperative learning Problem Based Learning |
Discussion of developing practical methods for the identification of new compounds | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)]
|
The accuracy of plotting and type
identification method |
5 |
| 15 | Able to propose chemical structures of unknown compounds based on their physical and chemical properties | Elucidation of the structure of organic compounds | Discovery learning
Cooperative learning Problem Based Learning |
The discussion integrates data on the physical and chemical properties of unknown compounds to predict chemical structures. | FF: 1 x (2 x 50″)
ST + SS: 1 x [(2 x 60″) + (2 x 60”)]
|
Accuracy of predicting chemical structure | 5 |
| 16 | Final exams | Written exam | 90 | The truth and completeness of the answer to the question | 50 | ||
| Total Rating | 100 | ||||||
Reference:
- Shriner,R.L., Herman, C.K.F., Morril, T.C., Curtin, D.Y., Fuson, R.C., 2004, The Systematic Identification of Organic Compounds 8th ed. John Wiley & Sons, Danvers, USA
- Chalmers R.A. 2014. Separation in Organic Chemistry. Chemistry Dept. University of Aberdeen, Old Aberdeen, Scotland
- Lab Series ANAL 0727, 2001, Identifiying an unknown compound by solubility, functional group test and spectral analysis
Glossary
GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study
