Sol Gel Chemistry

SEMESTER LEARNING PLAN

Document can be downloaded here

 

Course Title: Sol Gel Chemistry (Solgel)        

MK code: AKM21 468

Credit Weight: 2

Group of Courts: Elective

Semester: 6

Prerequisite Course: KAno2

 

Lecturer:

Dra. Sriyanti, M.Si

Dr. Choiril Azmiyawati, S.Si., M.Si

Graduate Learning Outcomes (GLO)

  Attitude GLO1-(S9) Demonstrate an attitude of being responsible for work in the field of expertise independently
Knowledge GLO2-(PP1) Mastering the theoretical concepts of structure, properties, changes, kinetics, and energetics of molecules and chemical systems, identification, separation, characterization, transformation, synthesis of micromolecular chemicals, and their application
GLO3-(PP3) Mastering the basic principles of software for analysis, synthesis, and molecular modeling in general or more specific chemical fields
General Skills GLO4-(KU1) Able to apply logical, critical, systematic, and innovative thinking in the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise
Special skill GLO5-(KK3) Able to analyze several alternative solutions in the fields of identification, analysis, isolation, transformation, and synthesis of available chemicals and present analysis conclusions for appropriate decision making

 

Course Description

In this course, students learn about the sol-gel process, the reactions involved, structural changes in the sol-gel process, the types of products produced, of the sol-gel process and its application in the development of encapsulation systems for both organic molecules and biomolecules.

 

Week Expected ability (Sub-CLO) Study Materials/ Learning Materials Learning methods Student Learning Experience Time (minutes) Evaluation
Criteria and Indicators %
1 Able to understand (C2), construct (P4), and discuss (A2) the Understanding and history of the Sol-Gel. Process Inter-molecular Interaction (BK8)/ Introduction (PB1)

 

a. Understanding of the sol-gel process

b. The history of sol-gel and its development

Discovery learning

Cooperative learning

Summarizing Information, asking (development, critique)

 

Searching, collecting, and compiling available Information to describe knowledge of the origin of the Sol-Gel process. Discuss and conclude the problems/tasks given by the lecturer in groups

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy in explaining the meaning of the Sol-Gel process

Accuracy describes the Sol-Gel Process and its Development with a minimum accuracy of 80%

5
2 Able to understand (C2), construct (P4), and discuss (A2) Non-Silicate Hydrolysis and Condensation Reaction Compound Reaction (BK7)/Non-Silicate Hydrolysis and Condensation Reaction (PB2)

a. Transition Metal

Discovery learning

Cooperative learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy explains the behavior of transition metals in hydrolysis and condensation reactions of non-silicate

with a minimum accuracy of 80%

10
3 Able to understand (C2), construct (P4), and discuss (A2) Non-Silicate Hydrolysis and Condensation Reaction Compound Reaction (BK7)/Non-Silicate Hydrolysis and Condensation Reaction (PB2)

b. Aluminate

c. Borate System

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy in explaining the hydrolysis and condensation reactions in aluminate

 

Accuracy describes the hydrolysis and condensation reactions in the borate system

5
4 Able to understand (C2), construct (P4), and discuss (A2) Non-Silicate Hydrolysis and Condensation Reaction Compound Reaction (BK7)/ Silicate Hydrolysis and Condensation Reaction (PB3)

a. Aqueous Silicate (Aqueous Silicate)

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy in explaining the Hydrolysis and Condensation Reactions of Aqueous Silicates 5
5 Able to understand (C2), construct (P4), and discuss (A2) Non-Silicate Hydrolysis and Condensation Reaction Compound Reaction (BK7)/ Silicate Hydrolysis and Condensation Reaction (PB3)

b. Silicon alkoxide

c. Multi Component Silicate

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy in explaining the hydrolysis and condensation reactions of silicon alkoxides

 

Accuracy in explaining the hydrolysis and condensation reactions of multi-component silicates

10
6 Able to understand (C2), construct (P4), and discuss (A2) Gel Forming Stages Inter-molecular Interaction (BK8)/ Gel Formation Stages (PB4)

a. Gelasi

b. Aging (aging)

c. Drying

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accurately describes the gelation process in the stages of gel formation

 

Accurately describes the aging process in the stages of gel formation

 

Accurately describes the drying process in the stages of gel formation

5
7 Able to understand (C2), construct (P4), and discuss (A2) structure evolution during consolidation Molecular Structure (BK5)/Evolution of Structure During Consolidation (PB5)

a. Porous Gel Structure: Serogel and airgel

b. Structure Change During Heating

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

accurately describes the structure of porous gels, aerogels, and angels

 

Accuracy describes the structural changes during heating

10
 

8

 

 

 

Midterm exam Written exam 90 The truth and completeness of the answer to the question
9 Able to understand (C2), construct (P4), and discuss (A2) Sol-Gel Application Molecular Structure (BK5)/Sol-Gel Application (PB6)

a. Thin Film and Coating

b. Monolith

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

accurately explains the manufacture and structure of Thin Films and Coatings

 

accurately explain the manufacture and structure of the Monolith

10
10 Able to understand (C2), construct (P4), and discuss (A2) Sol-Gel Application Molecular Structure (BK5)/Sol-Gel Application (PB6)

c. Fiber

d. Porous Gel and membrane

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy explains the manufacture and structure of the fiber

 

Accurately describes the fabrication and structure of porous gels and membranes

5
11 Able to understand (C2), construct (P4), and discuss (A2) Entrapping (Encapsulating) Organic Material Intermolecular Interaction (BK8)/Encapsulation (Encapsulation) of Organic Materials (PB7)

a. Production of ORMOSIL (Organic Modified Silica)

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy in explaining the process of making ORMOSIL (Organic Modified Silica) 10
12 Able to understand (C2), construct (P4), and discuss (A2) Entrapping (Encapsulating) Organic Material Intermolecular Interaction (BK8)/Encapsulation (Encapsulation) of Organic Materials (PB7)

b. Examples of making ORMOSIL

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy explains the examples of making ORMOSIL. 5
13 Able to understand (C2), construct (P4), and discuss (A2) Encapsulation of Biomolecules Inter-molecular Interaction (BK8)/ Encapsulation (Encapsulation) Biomolecules (PB8)

a. Encapsulation of proteins, antibodies, and vitamins

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy describes the process of encapsulation of proteins, antibodies, and vitamins 5
14 Able to understand (C2), construct (P4), and discuss (A2) Encapsulation of Biomolecules Inter-molecular Interaction (BK8)/ Encapsulation (Encapsulation) Biomolecules (PB8)

b. Examples of Encapsulation of proteins, antibodies, and vitamins

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy explains examples of Encapsulation of proteins, antibodies, and vitamins 5
15 Able to understand (C2), construct (P4), and discuss (A2) Encapsulation of Biomolecules Inter-molecular Interaction (BK8)/ Encapsulation (Encapsulation) Biomolecules (PB8)

c. Enzyme Encapsulation in Silica

d. Examples of enzyme encapsulation in silica

Discovery learning

Cooperative learning

Problem Based Learning

Summarizing Information, asking (development, critique)

Learn by digging/searching for Information (inquiry) and utilizing that Information to solve factual problems/designed by the lecturer

FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy describes the encapsulation of enzymes in silica

 

Accuracy describes examples of enzyme encapsulation in silica

10
16 Final exams Written exam 90 The truth and completeness of the answer to the question

 

Reference:

  1. Brinker, C.J. & Scherer, G. W., 1990, Sol-Gel Science, The Physics and Chemistry of Sol-Gel Processing, Academic Press, California
  2. Sumio Sakka, Sol-Gel Science and Technology, Processing, Characterization and Applications, Kluwer Academic Publisher, New York

Glossary

GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study

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