Chemical Separation (Pemkim)   

SEMESTER LEARNING PLAN

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Course Title: Chemical Separation (Pemkim)     

MK code: AKM21 347

Credit Weight: 2

Group of Courts: Compulsory

Semester: 4

Prerequisite Course: KA1,ENG, PKA

 

Lecturer:

Drs. Abdul Haris, Msi,

Dr. M. Cholid Djunaidi,MSi;

Gunawan, Msi, Ph.D

 

Graduate Learning Outcomes (GLO)

  Attitude GLO1-(S9) Demonstrate an attitude of responsibility for work in their field of expertise independently.
Knowledge GLO2-(PP1) Mastering the theoretical concepts of structure, properties, changes, kinetics, and energetics of molecules and chemical systems, identification, separation, characterization, transformation, synthesis of micromolecular chemicals, and their application.
GLO 3-(PP3) Mastering the basic principles of software for analysis, synthesis, and molecular modeling in general or more specific chemical fields.
General Skills GLO 4 -(KU1) Able to apply logical, critical, systematic, and innovative thinking in the context of the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise
Special skill GLO 5 -(KK3) Able to analyze several alternative solutions in identification, analysis, isolation, transformation, and synthesis of available chemicals and present analysis conclusions for appropriate decision making.

 

 

Course Description

In this course, students learn about: (a) introduction to separation methods commonly used by chemists. (b) The basic principles of physicochemical separation are molecular mass, molecular volume, molecular shape, dipole moment, electric charge, polarizability, and chemical reactivity (c). Students are expected to be able to distinguish the basic principles of separation methods. Students are also introduced to applying separation methods for mixtures of ions/molecules/organic compounds in waste, food, body, etc.

Week Expected ability (Sub-CLO) Study Materials/ Learning Materials Learning methods Student Learning Experience Time (minutes) Evaluation
Criteria and Indicators %
1 Able to understand (C2), construct (P4), and discuss (A2) Explain the principle of chemical separation, physicochemical separation and distinguish it from physical separation and provide several separation methods as examples Chemical separation theory, Physicochemical

a. chemical separation theory

b. Physicochemical Separation theory

Discovery learning

Cooperative learning

Search, collect and organize available information to describe the principles of separation of chemistry, physics-chemistry, physics, and examples. Discuss and conclude the problems/tasks given by the lecturer in groups. FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy explains the different principles of separation of chemistry, physics-chemistry, and physics. 5
2 Able to understand (C2), construct (P4), and discuss (A2) Principles of distillation theory 1 Introduction and principles of distillation theory

a. Principles of distillation theory

b. types of simple distillation, graded

Discovery learning

Cooperative learning

Discuss and conclude the problems/tasks given by the lecturer in groups FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

accuracy of explaining Principles of distillation theory: simple and graded distillation

 

 

5
3 Able to understand (C2), construct (P4), and discuss (A2) Principles of distillation theory 2 Introduction and principles of distillation theory

a. Principles of distillation theory

b. types of steam distillation, azeotropic distillation, etc.

Discovery learning

Cooperative learning

Problem Based Learning

Discuss and conclude the problems/tasks given by the lecturer in groups. FF: 1 x (2 x 50”)

ST + SS: 1 x [(2 x 50”) +

(2 x 60”)]

Accuracy of explaining Principles of distillation theory; steam distillation, azeotrope, etc. 5
4 Able to understand (C2), construct (P4), and discuss (A2) solvent extraction theory 1 Solvent extraction separation theory

a. solvent extraction theory (plate theory)

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

– the accuracy of explaining the theory of solvent extraction

– accuracy in explaining solvent extraction theory (plate theory)

– Explain the magnitude of Kd (distribution coefficient) and D

10
5 Able to understand (C2), construct (P4), and discuss (A2) solvent extraction theory 2 solvent extraction separation theory

a. types of solvent extraction

b. solvent extraction for metals

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

– the accuracy of explaining the types of solvent extraction

– accurately describes solvent extraction for metals

5
6 Able to understand (C2), construct (P4), and discuss (A2) Chromatography

chromatographic separation theory

chromatographic separation theory

a. Chromatographic theory

b. chromatograph components

c. types of chromatography

d. adsorption chromatography

e. gas-liquid chromatography

f. ion-exchange chromatography

g. other chromatography

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

– the accuracy of explaining the theory of chromatography

– the accuracy of explaining the components in chromatography

– the accuracy of explaining the types of chromatography

– accuracy of explaining adsorption chromatography, liquefied gas, ion exchange

-precision explains another principle of chromatography.

10
7 Able to understand (C2), construct (P4), and discuss (A2) membranes

 

membrane separation theory

a. membrane definition

b. organic membrane

c. inorganic membrane

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

-precisely explain membrane principle

-precisely explain the principle of organic membranes

-precisely explain the principle of inorganic membranes

5
8 Written exam 90
9 Able to understand (C2), construct (P4), and discuss (A2) electrochemistry 1 electrochemical separation theory 1

a. electrochemical separation with potential control

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

-precisely explain the theory of electrochemical separation 10
10 Able to understand (C2), construct (P4), and discuss (A2) Electrochemical theory 2 electrochemical separation theory 1

a.                   electrochemical separation with potential control

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

-precisely explain the theory of electrochemical separation of potential control 5
11 Able to understand (C2), construct (P4), and discuss (A2) Electrochemical theory 3

 

electrochemical separation theory 1

a.                   electrochemical separation with constant potential

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

-precisely explain the theory of electrochemical separation

-accurately explain the theory of fixed potential electrochemical separation

5
12 Able to understand (C2), construct (P4), and discuss (A2)  electrogravimetry 1 electrogravimetric separation theory 1

a.  electrogravimetric separation, principles

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

-precisely explain the principle of electrogravimetry 10
13 Able to understand (C2), construct (P4), and discuss (A2)  electrogravimetry 2 electrogravimetric separation theory 2

b. electrogravimetric application for separation

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

-accurately explain the application of electrogrvimetry 10
14 Able to understand (C2), construct (P4), and discuss (A2) the principle of electrophoresis electrogravimetric separation theory 2 Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve real problems/designed by lecturers. FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

M43 electrophoresis principle 10
15 Able to understand (C2), construct (P4), and discuss (A2) electrophoresis applications for separation

electrophoretic separation theory

–                     Electrophoresis application for separation

Discovery learning

Cooperative learning

Problem Based Learning

Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by lecturers with accuracy in explaining FF: 2 x 50

ST: 2 x 60

SS: 2 x 60

electrophoresis application for separation 5
16 Final exams Written exam 90 The truth and completeness of the answer to the question
Total Rating 100

 

Reference:

  1. Kriz, PL,. Introduction to Organic Laboratory Technique
  2. Sudjadi, 1990, Metode Pemisahan
  3. Khopkar, 1990, Kimia Analitik Dasar
  4. Mulder, M, 1996, Basic Principle of Membrane Technology, Kluwer Academic Publisher
  5. Skoog, 1997, Principle of Instrumental Analytical
  6. Bartsch, Way, 1996, Chemical Separations with Liquid Membranes, C.S. Symposium Series
  7. Several journals

 

Glossary

 

GLO = Graduate Learning Outcome

CLO = Course Learning Outcomes

FF = Face to Face Learning

ST = Structured tasks

SS = Self Study

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