SEMESTER LEARNING PLAN
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Course Title: Non-aqueous Analytical Chemistry (KANA)
MK code: AKM21 552
Credit Weight: 2
Group of Courts: elective
Semester: 5
Prerequisite Course: KRX, KAI1
Lecturer:
Drs. Abdul Haris, M.Si.,
Didik Setiyo W., S.Si., M.Si.
Graduate Learning Outcomes (GLO)
| Attitude | GLO1-(S9) | Demonstrate an attitude of responsibility for work in their field of expertise independently. |
| Knowledge | GLO2-(PP2) | Mastering complete operational knowledge of functions, how to operate standard chemical instruments, as well as analysis of data and information from instruments |
| General Skills | GLO3-(KU1) | Able to apply logical, critical, systematic, and innovative thinking in the context of the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise |
| GLO 4 -(KU2) | Able to demonstrate independent, quality, and measurable performance | |
| GLO 5 -(KU7) | Able to be responsible for achieving group work results and supervising and evaluating the completion of work assigned to workers under their responsibility | |
| Special Skills | GLO 6 -(KK3) | Mastering complete operational knowledge of functions, how to operate standard chemical instruments, and analysis of data and information from these instruments |
Course Description
This course will offer other alternatives for the solute, acid-base solvation media, solute-solvent interactions, and the advantages of non-aqueous media in solving analytical and synthesis problems and applying science chemistry technology. Students can identify solute-solvent interactions to select non-aqueous media in various approaches to solve chemical analysis and synthesis problems and construct ways to measure parameters in chosen media.
| Week | Expected ability (Sub-CLO) | Study Materials/ Learning Materials | Learning methods | Student Learning Experience | Time (minutes) | Evaluation | |
| Criteria and Indicators | % | ||||||
| 1 | Students can understand (C2), develop (P4), and discuss (A2) about non-aqueous methods/systems compared to aqueous systems | Introduction to non-aqueous systems (BK 16)
a. solute-solvent system b. non-aqueous type of solute c. non-aqueous solvent type d. intermolecular interactions |
Discovery learning
Cooperative learning |
Students listen, take notes and ask questions about the subject.
1) Students form small groups and discuss solute-solvent systems, types of non-aqueous solutes, types of non-aqueous solvents, and molecular interactions 2) Students work on practice questions and present the results, |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in understanding about solvent solutes in non-aqueous media | 2,5 |
| 2-3 | Students can apply (C3), construct (P4), and discuss (A2) non-aqueous concepts and phenomena in supporting the application of non-aqueous analytical methods without opening notes at least 80% correct. | Characteristics of non-aqueous systems (BK 16)
a. Solvation system b. non-water system characteristics c.Classification of solvent d. Hydrogen bond e. Non-water system |
Discovery learning
Cooperative learning |
Students listen, take notes and ask questions about the subject.
1) Students form small groups and discuss solvation systems, characteristics of non-aqueous systems, classification of solvents, hydrogen bonds, and non-aqueous systems. 2) Students work on practice questions and present the results, |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in understanding various water solvents, molecular interactions, and solvation systems | 2,5 |
| 4-5 | Students can understand (C2), construct (P4), and discuss (A2) the theory of acid-base in aqueous media to non-aqueous acids and bases without opening notes at least 80% correct. | Acid-Base in non-aqueous media
a. Arrhenius Theory b. Bronsted-Lowry theory c. Lewis theory d. Usanovich Teori theory e . pH interpretation |
Discovery learning
Cooperative learning small group discussion |
1) Students listen, take notes, ask questions about the subject, and discuss the Arrhenius Theory, Bronsted-Lowry Theory, Lewis Theory, Usanovich Theory, and pH interpretation in small groups.
2) Students work on practice questions about acid-base theory in non-aqueous media 3) Students make conclusions on the results of their work. |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in understanding the theory of acid-base in non-aqueous solvent media, which is interpreted by measuring pH. | 5 |
| 6-7 | Students can apply (C3), construct (P4), and discuss (A2) acid-base analysis of non-aqueous media without opening notes at least 80% correct. | Acid-base titration in medium
a.- Base Titration b. Acid Titration c. Acid-base balance |
Discovery learning
Cooperative learning small group discussion |
1) Students listen, take notes and ask questions about the subject, discuss in small groups to understand Base Titration, Acid Titration, and Acid-base Balance
2) Students work on practice questions and present the results, 3) Students make conclusions on the results of the discussion above |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in acid-base titration and chemical equilibrium | 5 |
| 8
|
Mid-semester | Written exam | 90 | The truth and completeness of the answer to the question | 35 | ||
| 9-10 | Students can describe (C2) and apply (C2) thermodynamic properties, analyze emf measurements (C4) with the application of Emf data without opening notes at least 80% correct. | Thermodynamic properties
a. Reference electrode in non-aqueous solvent b. Electrode potential and its relation to non-aqueous selective solvents |
Discovery learning
Cooperative learning Problem Based Learning |
1) Students listen, take notes, and ask questions about the subject. thermodynamic properties
2) Students work on practice questions about electrode potential and its relation to non-aqueous selective solvents. 3) Students make conclusions on the work of evaluating the results above |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in understanding thermodynamic properties, electrode potential concerning | 5 |
| 11-12 | Students can understand (C2) the concept of the rate and mechanism of several organic compounds and the relationship between half-cell potential and the properties of aromatic hydrocarbons, analyze (C4) with voltammetry without opening notes at least 80% correct | Electrode Process
1. Rates and mechanisms of some organic compounds 2. The relationship between half-cell potential and the properties of aromatic hydrocarbons 3. Reduction of oxygen and hydrogen 4. Study of ion solvation voltammetry |
Discovery learning
Cooperative learning small group discussion |
1) Students listen, take notes, and ask questions about the subject of the electrode process.
2) Students work on practice questions and present the results Students form small groups and discuss statistical tests on non-parametric data. |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in understanding the processes that occur at the electrode | 5 |
| 13-15 | Students can apply (C2) Application of non-aqueous ion solvation for hydrometallurgy including solvent extraction and to analyze (C4) separation of copper, silver, and lead Electrowinning, Electrorefining of metals from non-aqueous solutions correctly at least 80% | Application of non-aqueous ion solvation for hydrometallurgy
a. Separation of copper, silver, and b. Electrowinning c..Electrorefining d. Non-aqueous battery electrolyte e. Metal electrodeposition |
Discovery learning
Cooperative learning small group discussion |
1) Students listen, take notes, and ask questions about non-aqueous ion solvation for hydrometallurgy, including extraction
solvent. 2) Students work on practice questions and present the results, 3) Students discuss completing assignments 4) Students make conclusions on the work above |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Accuracy in the application of non-aqueous ion solvation for hydrometallurgy
The truth of the conclusion based on the data |
5 |
| 16 | Final exams | Written exam | 90 | The truth and completeness of the answer to the question | 35 | ||
| Total Rating | 100 | ||||||
Reference:
- Popovich, C. dan Tomkins, RPT, Nonaqueous Solution Chemistry, 1981, John Wiley and Sons, New York
- Kenneth, J.H., 1990, Analitycal Chemistry: Principles, Edisi ke-2, Saunders College Pub., New York
Glossary
GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study
