SEMESTER LEARNING PLAN
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Course Title: Instrumental Analytical Chemistry 1 (KAI 1)
MK code: AKM21 342
Credit Weight: 2
Group of Courts: Compulsory
Semester: 4
Prerequisite Course: KA2, ENG
Lecturer:
Drs. Abdul Haris, M.Si.,
Didik Setiyo W., S.Si., M.Si.,
Graduate Learning Outcomes (GLO)
| Attitude | GLO1-(S9) | Demonstrate an attitude of responsibility for work in their field of expertise independently. |
| Knowledge | GLO2-(PP2) | Mastering complete operational knowledge of functions, how to operate standard chemical instruments, as well as analysis of data and information from instruments |
| General Skills | GLO 3 -(KU2) | Able to demonstrate independent, quality, and measurable performance |
| Special Skills | GLO 4 -(KK1) | Able to generate appropriate conclusions based on the results of the interpretation of chemical analysis that has been carried out. |
| GLO 5 -(KK3) | Mastering complete operational knowledge of functions, how to operate standard chemical instruments, and analysis of data and information from these instruments |
Course Learning Outcomes
| CLO-1 | Students can rationalize (C4) the most suitable instrumental analysis method in solving (C4) problems based on spectrometry and microscopy and can develop/modify (A4) new systems to obtain reliable chemical quantization. |
Course Description
This course provides basic instrumental analysis skills and applies them to real-life examples. The basic concepts of spectrometric analysis are given in detail for each. The instrumental approach explained, starting from the interaction of electromagnetic radiation with matter, the laws that underlie the process, and each instrument’s essential components displayed. The sample preparation technique until the application of spectral interpretation of the data obtained is described to students. The same approach is also introduced on the surface analysis of the sample microscopically.
| Week | Expected ability (Sub-CLO) | Study Materials/ Learning Materials | Learning methods | Student Learning Experience | Time (minutes) | Evaluation | |
| Criteria and Indicators | % | ||||||
| 1 | Students can understand (C2) the basic concepts of spectrometric analysis and detail (C3) the phenomenon of the interaction of matter-energy in the application of instrumental analysis correctly at least 80% | BK16. Introduction to Spectrometry (PB1)
a. The nature of electromagnetic radiation b. Interaction of energy and matter c. The basic laws of spectrometric analysis |
Discovery learning
Cooperative learning |
Students listen, take notes and ask questions about the subject
Students respond to feedback in interactive lecture sessions and summarize the conclusions of the interaction |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
||
| 2 | Students can understand (C2) component systems and detail (C4) their functions in a complete set of tools correctly at least 80% | BK16. Optical spectroscopic instrument system (BP2)
a. Types of optical methods b. Radiation source c. Monochromator d. Sample place e. Detector f. Signal processing and reading system g. Instrumentation system design |
Discovery learning
Cooperative learning |
Students listen, take notes and ask questions about the subject
Students are active in group discussions |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
||
| 3 | Students can describe (C2) the quantitative formulation of measurement perfectly and relate (C3) with some of the spectrometric methods discussed | BK16. Absorption Spectrometry (BP3)
a. Quantitative aspects of absorption measurement b. A term used in absorption measurement c. Some absorption spectrometry techniques |
Discovery learning
Cooperative learning Problem Based Learning |
Students listen, take notes and ask questions about the subject
Students practice various quantitative relationships of absorption measurement quantities |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
The answer to the question is correct | 2,5 |
| 4 | Students can detail (C3) the instrument design system, rationalize (C4) the measurement phenomenon and solve the problem (P4) of mixed samples correctly at least 80% | BK16. UV-Vis Spectrometry (BP4)
a. Molar absorptivity b. Components of UV-Vis spectrometry instrumentation c. Qualitative and quantitative analysis d. Analyte mixture analysis |
Discovery learning
Cooperative learning small group discussion |
Students listen, take notes and ask questions about the subject
Students practice qualitative and quantitative questions both single and mixed samples |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
||
| 5-6 | Students can understand (C2) the basic concepts of AAS and atomic transitions, examine (C4), and evaluate (C5) the AAS analysis system correctly at least 80% | BK16. Atomic Absorption Spectrophotometry (BP5)
a. Atomic spectroscopy theory b. Atomization system with flame c. Flameless atomization system d. AAS instrumentation system e. Interference with AAS measurements f. Analysis Techniques |
Discovery learning
Cooperative learning small group discussion |
Students listen, take notes and ask questions about the subject
Students actively discussing Students practice solving analytical problems due to interference and presenting the results of discussions with group presentations. |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Activeness in discuss | 5 |
| 7 | Students can describe (C2) the principle of the method and explain the application (A5) of the method in a broader context | BK15 and BK16. FTIR Spectroscopy (BP6)
a. Infrared absorption theory b. FTIR spectroscopic instrument components c. Sample handling d. Qualitative and quantitative analysis e. Spectral regions are essential for analysis by FTIR |
Discovery learning
Cooperative learning small group discussion Problem Based Learning |
Students listen, take notes and ask questions about the subject
Students actively discussing Students practice dealing with real problems in determining functional groups and quantitative sides of FTIR analysis |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Activeness in discuss | 5 |
| 8
|
Mid-semester | Written exam | 90 | The truth and completeness of the answer to the question | 37,5 | ||
| 9-10 | Students can understand (C2) the principle of atomic emission spectroscopy and understand the application of the (P2) method to specific samples | BK16. Emission Spectroscopy (BP7)
a. Spectra with high energy sources b. Plasma emission spectroscopy (ICP) c. Plasma spectroscopic instrumentation d. Quantitative analysis with ICP |
Discovery learning
Cooperative learning Problem Based Learning |
Students listen, take notes and ask questions about the subject
Students dissect related international journals |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Activeness in discuss | 5 |
| 11 | Students can compare (C2) the application of the surface analysis approach with other methods | BK15. Surface Analysis (BP8)
a. Introduction to material characterization b. Variety of probes on surface analysis |
Discovery learning
Cooperative learning small group discussion |
Students listen, take notes and ask questions about the subject. | FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Activeness in discuss | 5 |
| 12-14 | Students can take advantage of the application of the (C3) SEM analysis method for samples and correctly predict (C5) the composition of the material surface from the analysis data at least 80% | BK15 and 16. Scanning Electron
Microscopy(SEM) (PB9) a. Introduction to analysis with SEM b. Instrumentation system on SEM c. SEM working principle d. Electron transition in SEM analysis e. SEM App f. SEM-EDS |
Discovery learning
Cooperative learning small group discussion |
Students listen, take notes and ask questions about the subject
Students dissect related international journals |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Activeness in discuss | 5 |
| 15 | Students can take advantage of the application of the (C3) TEM analysis method and be able to compare (A4) with the SEM method correctly at least 80% | BK15 and BK16. Transmission Electrons
Microscopy(TEM) (PB10) a. Introduction to analysis with TEM b. Instrumentation system on TEM c. TEM working principle d. Electron transition in TEM analysis e. TEM app |
Discovery learning
Cooperative learning small group discussion |
Students listen, take notes and ask questions about the subject
Students practice critically making image comparisons analysis |
FF: 1 x (2 x 50”)
ST + SS: 1 x [(2 x 50”) + (2 x 60”)] |
Activeness in discuss | 2,5 |
| 16 | Final exams | Written exam | 90 | The truth and completeness of the answer to the question | 37,5 | ||
| Total Rating | 100 | ||||||
Reference:
- Skoog, D.A. 1985, Principles of Instrumental Analysis, edisi ke-3, Saunders College Pub., Philadelphia
- Skoog, D.A., West, D.M., dan Holler, F.J., 1994, Analytical Chemistry: An Introduction, edisi ke-6, Saunders College Pub. , Philadelphia
Glossary
GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study
