SEMESTER LEARNING PLAN
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Course Title: Thermal Analysis (AnTer)
MK code: AKM21 447
Credit Weight: 2
Group of Courts: Elective
Semester: 4
Prerequisite Course: KA2, KAI1
Lecturer:
Dr. Retno Ariadi L., M.Si
Gunawan, M.Si., Ph.D
Graduate Learning Outcomes (GLO)
| Attitude | GLO1-(S9) | Demonstrate an attitude of responsibility for work in their field of expertise independently. |
| Knowledge | GLO2-( PP2) | Mastering complete operational knowledge of functions, operating standard chemical instruments, and analyzing data and information from these instruments |
| General Skills | GLO 3 -(KU1) | Able to apply logical, critical, systematic, and innovative thinking in the development or implementation of science and technology that pays attention to and uses humanities values by their field of expertise. |
| GLO 4 -(KU2) | Able to demonstrate independent, quality, and measurable performance. |
Course Description
In this course, students learn about: quantitative gravimetric analysis (precipitation and volatilization) with a quantitative approach instrument to measure thermal stability. The system consists of several lessons thermogravimetric analysis (TGA), differential thermal analysis (DTA), differential scanning calorimetry (DSC), and dilatometry.
| Week | Expected ability (Sub-CLO) | Study Materials/ Learning Materials | Learning methods | Student Learning Experience | Time (minutes) | Evaluation | |
| Criteria and Indicators | % | ||||||
| 1 | Able to understand (C2), construct (P4), and discuss (A2) the basic principles of thermal analysis theory | Introduction the basic idea of thermal analysis | Discovery learning
Cooperative learning |
Summarizing information
Asking (development, critique) search, collect, and collate existing information to describe knowledge of the Origins of quantum mechanics Discuss and conclude the problems/tasks given by the lecturer in groups. |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
accuracy explains the definition of thermal analysis | 10 |
| 2-3 | Able to understand (C2), construct (P4), and discuss (A2) the basic principles of thermal gravimetric analysis | Introduction and principles of TGA theory
Introduction to TGA; sample preparation procedure, tool use procedure, factors |
Discovery learning
Cooperative learning |
listen,
write ask Discuss and conclude the problems/tasks given by the lecturer in groups. |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
the accuracy of explaining the Principles of TGA theory | 5 |
| 4 | Able to understand (C2), construct (P4), and discuss (A2) reading thermal gravimetric analysis data | application theory
a. Acid-base titration reaction |
Discovery learning
Cooperative learning Problem Based Learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
– the accuracy of explaining the data analysis of the TGA curve
– the accuracy of reading the data to solve the questions given |
5 |
| 5-6 | Able to understand (C2), construct (P4), and discuss (A2) differential thermal analysis methods | DTA theory
Thermal thermodynamic aspects; DTA curve data |
Discovery learning
Cooperative learning Problem Based Learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
– the accuracy of explaining the basic principle formulations of DTA
– the accuracy of using DTA to solve the questions given |
5 |
| 7 | Able to understand (C2), construct (P4), and discuss (A2) TGA analysis methods | Synchronization of analytical data based on the theory of TGA, DTG and DTA | Discovery learning
Cooperative learning Problem Based Learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
– the accuracy of explaining the basic principle formulations of the gravimaterial method by instrument and using data from the instrument | 10 |
| 8 | Midterm exam | 1-7 meeting | – | Written exam | 90 | – | |
| 9-10 | Able to understand (C2), construct (P4), and discuss (A2) the differential scanning calorimetry (DSC) method | Construction and theory of differential scanning calorimetry (DSC) method | Discovery learning
Cooperative learning Problem Based Learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
-precisely explains the basic principles, calculations, and applications of DSC data
-accuracy of using the formulas given to solve questions about DSC |
10 |
| 11-12 | Able to understand (C2), construct (P4), and discuss (A2) the dilatometry method | DSC basic principles, influence factors, instruments, curve data | Discovery learning
Cooperative learning Problem Based Learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
-accuracy of explaining dilatometry
-the accuracy of using the formulas given to solve problems about dilatometry |
10 |
| 13-14 | Able to understand (C2), construct (P4), and discuss (A2) methods of using DSC and dilatometry on samples | Processing data based on raw data from DSC, DTA, TG theory | Discovery learning
Cooperative learning Problem Based Learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
-precisely explain the theory of thermal instrument alloys
-accuracy of using the formulas given to solve problems about thermal instruments |
10 |
| 15 | Able to understand (C2), construct (P4), and discuss (A2) methods of analyzing inorganic compounds using thermal instruments | application to the properties of alumina |
Discovery learning Cooperative learning Problem-based learning |
listen,
write ask Learn by digging/searching for information (inquiry) and utilizing that information to solve factual problems/designed by the lecturer |
FF: 2 x 50
ST: 2 x 60 SS: 2 x 60 |
-precisely explains the basic principles of thermal instruments
– the accuracy of using the formulas given to solve problems about the principle of thermal instruments |
10 |
| 16 | Final exams | Meeting 9-15 | – | Written exam | 90 | The truth and completeness of the answer to the question | – |
| Total Rating | 100 | ||||||
Reference:
- Dodd, J.W. dan Tonge, K.H., 1987, Analytical chemsitry by open learning, Thermal anlsysis.
- Ehrenstein G, Riedel, Trawiel, 2004, Thermal analysisi of plastic, Hanse
Glossary
GLO = Graduate Learning Outcome
CLO = Course Learning Outcomes
FF = Face to Face Learning
ST = Structured tasks
SS = Self Study
